Substitution of sulfochromatic mixtures

Number

182-EN

Section

General Section

Use

Sector

Scientific research and development

Function

Cleaning agent

Process

Manual activities involving hand contact

Product category

washing ad cleaning products

Application

Cleaning of Laboratory materials

Abstract

This document proposes and analyses different alternatives to sulfochromatic mixtures (chrome VI) in the cleaning of laboratory instruments. The full text is only available in French.

Substituted substances

Chromium (VI) compounds, with the exception of barium chromate and of compounds specified elsewhere in this Annex

CAS No. EC No. Index No. 024-017-00-8

Chemical group

Chromium compounds

Classification: hazard statements

H350i May cause cancer by inhalation
H317 May cause an allergic skin reaction
H400 Very toxic to aquatic life
H410 Very toxic to aquatic life with long lasting effects

Other adverse effects

The substance is: 1 carcinogen (IARC: chromium VI compounds), as listed in the Substance Database according to SUBSPORT Screening Criteria (SDSC).

Sulphuric acid

CAS No. 7664-93-9 EC No. 231-639-5 Index No. 016-020-00-8

Chemical group

Inorganic acid

Classification: hazard statements

H314 Causes severe skin burns and eye damage

Other adverse effects

Strong inorganic acid mists: 1 carcinogen (IARC) as listed in the Substance Database according to SUBSPORT Screening Criteria (SDSC).

Alternative Substances

Non ionic surfactants

CAS No. EC No. Index No.

Chemical group

Surfactants

Potassium hydroxide

CAS No. 1310-58-3 EC No. 215-181-3 Index No. 019-002-00-8

Chemical group

Potassium compounds; hydroxides

Classification: hazard statements

H302 Harmful if swallowed
H314 Causes severe skin burns and eye damage

Sodium hydroxide

CAS No. 1310-73-2 EC No. 215-185-5 Index No. 011-002-00-6

Chemical group

Sodium compounds; hydroxides

Classification: hazard statements

H314 Causes severe skin burns and eye damage

Reliability of information

Evidence of assessment: there is evidence of an official (positive) assessment of the substitution

Reason substitution

CMR
other toxic effects
neurotoxicant

Hazard Assessment

Substance to be substituted: Sulfochromatic mixtures may cause cancer by inhalation, is very toxic to aquatic life, is very toxic to aquatic life with long lasting effects and may cause an allergic skin reaction. The substance is a category 1B carcinogen (CLP Regulation) and a sensitiser (H317, H334; CLP Regulation), Sulphuric acid causes severe skin burns and eye damage. Alternative substances: Potassium hydroxide causes severe skin burns and eye damage and is harmful if swallowed. Non-ionic surfactants have no harmonised classification according to Annex VI of Regulation (EC) No 1272/2008 (CLP Regulation). Sodium hydroxide causes severe skin burns and eye damage. The substances are not listed in the Substance Database according to SUBSPORTplus Screening Criteria (SDSC). These detergents are strongly alkaline and corrosive and are irritating to skin, even after dilution. Whatever the form used (powder or solution), safety measures and protective equipment (glasses, gloves…) need to be taken

Description of Substitution

Sulfochromatic mixtures (K2Cr2O7, Na2Cr2O7… in concentratedsulphuric acid, H2SO4) are still regularly used in laboratories for the cleaning of glass flasks and vessels. The mixture is considered highly hazardous to human health: Chromium VI salts are classified as human carcinogens categories 1 and 2 by the EU and their use in laboratories must be banned. This article presents a number of solutions for the substitution of sulfochromatic mixtures which include: -Decon 90 (VWR International): An emulsion of anionic and non-ionic surface active agents, caustic soda and stabilizing agents -TFD 4 (Franklab): a mixture Anionic and non-ionic surfacting agents, potassium hydroxide andstabilizing agents -Alconox (Vasse Industries): Anionic surfacting agents These are detergents with tenso-active agents, like alkyl benzenesulfonates, that can be used for cleaning laboratory instrument. These detergents are also available for cleaning with ultrasonic baths.

Case/substitution evaluation

Chromium VI is a highly toxic substance included in SUBSPORTplus’s Priority list for substitution. Alternatives imply less health hazards. Alternative products are not exempt for risks but avoid the handling and dispersion of a product highly genotoxic that implies higher risks.

Type of information supplier

Research

Further information

Material Safety Data Sheet, detergent Decon90

Type of publication and availability

freely available (in French)

Publication source: author, company, institute, year

Le remplacement du mélange sulfochromique Brigitte Diers, Frédérique Mazé-Coradin Magazine: L’actualité chimique http://www.lactualitechimique.org/ 2004

Publication source

Type of publication and availability

https://www.lactualitechimique.org/Le-remplacement-du-melange-sulfochromique

Date, reviewed

November 26, 2021